BIS(TRIMETHYLSILYL)-N-TERT-BUTYLACETALDIMINE合成路线 (共 14 条)
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-60°C; 5 h;
参考文献
Buffa; Zahradnik; Foltinova
Heterocyclic Communications, 2001 , vol. 7, # 4 p. 331 - 336
反应条件
1: 1) LDA / 1) THF, -60 deg C, 20 h, 2) -60 deg C, 2h 2: 1) LDA / 1) THF, -60 deg C, 5 h, 2) -60 deg C, 45 min View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2517 - 2522
反应条件
lithium diisopropyl amide 1) THF, -60 deg C, 5 h, 2) -60 deg C, 45 min; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2517 - 2522
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 2.5 h, 2) ether, water, RT, 1 h; Yield given. Multistep reaction;
参考文献
Bellassoued, Moncef; Majidi, Assieh
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2517 - 2522
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 5 h, 2) ether, water, RT, 1 h; Yield given. Multistep reaction;
参考文献
Bellassoued, Moncef; Majidi, Assieh
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2517 - 2522
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 4.5 h, 2) ether, water, RT, 1 h; Yield given. Multistep reaction;
参考文献
Bellassoued, Moncef; Majidi, Assieh
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2517 - 2522
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Yield given;
参考文献
Tetrahedron Letters, , vol. 31, # 3 p. 349 - 352
反应条件
zinc(II) chloride; zinc dibromide other aldehydes, E/Z-isomers; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2517 - 2522
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 6 h, 2) ether, water, RT, 1 h; Yield given. Multistep reaction;
参考文献
Bellassoued, Moncef; Majidi, Assieh
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2517 - 2522
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 3 h, 2) ether, water, RT, 1 h; Yield given. Multistep reaction;
参考文献
Bellassoued, Moncef; Majidi, Assieh
Journal of Organic Chemistry, 1993 , vol. 58, # 9 p. 2517 - 2522