dirhodium(II) tetraoctanoate in 1,2-dichloro-ethane T=70°C; 16 h; Inert atmosphereMolecular sieve;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '2048025', constants.ctx, '0')">trifluoromethanesulfonyl azide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '4933678', constants.ctx, '0')">copper(II) sulfate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />T=20&deg;C;&nbsp;&nbsp;Inert atmosphere;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide / 1,4-dioxane; water / 12 h / 80 &deg;C / Inert atmosphere<br />2: trifluoromethanesulfonyl azide; copper(II) sulfate; triethylamine / methanol; dichloromethane; water / 20 &deg;C / Inert atmosphere<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 2,6-di-tert-butyl-pyridine / 1,2-dichloro-ethane / 2 h / 70 &deg;C / Inert atmosphere<br />2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide / 1,4-dioxane; water / 12 h / 80 &deg;C / Inert atmosphere<br />3: trifluoromethanesulfonyl azide; copper(II) sulfate; triethylamine / methanol; dichloromethane; water / 20 &deg;C / Inert atmosphere<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 1,4-dioxane / 12 h / 100 &deg;C / Inert atmosphere<br />2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide / 1,4-dioxane; water / 12 h / 80 &deg;C / Inert atmosphere<br />3: trifluoromethanesulfonyl azide; copper(II) sulfate; triethylamine / methanol; dichloromethane; water / 20 &deg;C / Inert atmosphere<br /> <br /> &nbsp;