二甲基二硫代氨基甲酸钠合成路线 (共 123 条)
反应条件
in methanol
9 h; Ambient temperature;
参考文献
Tsuboi, Sadao; Kohara, Noriyuki; Doi, Katsumi; Utaka, Masanori; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3205 - 3210
反应条件
sodium hydroxide
20 h;
参考文献
Gueguen; Boisde; Queffelec; Haelters; Thouvenot; Corbel; Nodet
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 10 p. 4492 - 4499
反应条件
(i) EtOH, (ii) aq. HCl; Multistep reaction;
参考文献
Garraway,J.L.
Journal of the Chemical Society, 1962 , p. 4072 - 4076
参考文献
Roessler and Hasslacher Chem.Co.
Patent: US1798588 , 1926 ;
Full Text Show Details
Roessler and Hasslacher Chem.Co.
Patent: US1780545 , 1928 ;
反应条件
in water
byproducts: [N(CH3)2CSS]2; RuCl3 was added to aq. soln. Me2NCS2Na (1:3); ppt. was filtered off, washed with water and dried in vacuo over P2O5, prep. column chromy. on silica; elem. anal.;
参考文献
Giovagnini, Lorena; Sitran, Sergio; Castagliuolo, Ignazio; Brun, Paola; Corsini, Maddalena; Zanello, Piero; Zoleo, Alfonso; Maniero, Annalisa; Biondi, Barbara; Fregona, Dolores
Dalton Transactions, 2008 , # 47 p. 6699 - 6708
反应条件
in not given
pptn. of K2(RuCl6) soln. with Na-dialkyldithiocarbamate in coldness;;
参考文献
Malatesta, L.
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 195 - 198
Full Text Show Details
Gmelin Handbook: Ru: SVol., 173, page 469 - 471
参考文献
D'Amico,J.J. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3564 - 3568
参考文献
Yanagawa, Makato; Moriya, Osamu; Watanabe, Yoshihiko; Ueno, Yoshio; Endo, Takeshi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 2203 - 2204
反应条件
2,4,6-Triphenylpyridine
T=160°C; P=1 Torr; 0.5 h;
参考文献
Katritzky, Alan R.; Rezende, Marcos C.; Thind, Sukhpal S.
Journal of Chemical Research, Miniprint, 1980 , # 9 p. 4031 - 4040
参考文献
Gur'janowa; Kusina
Zhurnal Fizicheskoi Khimii, 1956 , vol. 30, p. 616,621
Chem.Abstr., 1956 , p. 14292