二甲基二硫代氨基甲酸钠合成路线 （共 123 条）
反应条件
in chloroform at room temp. for 2 h, concg.;
参考文献
Kupchik, E. J.; Calabretta, P. J.
Inorganic Chemistry, 1965 , vol. 4, p. 973 - 978
参考文献
Nachmias
Annales de Chimie (Cachan, France), 1952 , vol. <12> 7, p. 584,599
反应条件
(i) NaOEt, EtOH, (ii) /BRN= 3569024/, benzene; Multistep reaction;
参考文献
Pluijgers,C.W.; Van Der Kerk,G.J.M.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 1089 - 1100
反应条件
in chloroform at room temp.;
参考文献
Kupchik; Theisen
Journal of Organometallic Chemistry, 1968 , vol. 11, p. 627
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Gmelin Handbook: Sb: Org.Comp.2, 1.3.1.1.11, page 135 - 137
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Theisen, C. T.
Diss. Abstr. B, Diss. St. John's Univ. 1967, pp. 1/90 1968 , vol. 28, p. 3660
参考文献
Hooker Chem.Corp.
Patent: US3651129 , 1972 ;
Chem.Abstr., 1972 , vol. 76, # 153394
Full Text Show Details
Hooker Chem.
Patent: US3825582 , 1974 ;
Chem.Abstr., 1974 , vol. 81, # 77695
反应条件
in dichloromethane Kinetics; React. of starting complexes (CH2Cl2, 12 h, room temp., anhydrous conditions, dry Ar).; Crystn. from CH2Cl2 under hexane (-15°C), elem. anal., variable-temp. NMR spectroscopy.;
参考文献
Femec, Douglas A.; Silver, Michael E.; Fay, Robert C.
Inorganic Chemistry, 1989 , vol. 28, p. 2789 - 2796
反应条件
in chloroform 1 h, 25°C; recrystd. from CH3CN;
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 627
Bi: Org.Verb., 1.5.1.2.5, page 129 - 130
Diss. Abstr. B, Dissert. St. John's Univ. 1968 , vol. 28, p. 3660/1
反应条件
in chloroform 1h at 25°C;
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 627
Bi: Org.Verb., 1.3.3.2.4.1, page 62 - 68
反应条件
in dichloromethane Kinetics; Stirring of mixt. of starting complexes in CH2Cl2 at reflux under anhydrous conditions in a dry Ar atmosphere (24 h).; Filtn. of react. mixt., removal of solvent by trap-to-trap distn., crystn. of crude resulting material from CH2Cl2 under hexane, elem. anal., variable-temp. NMR spectroscopy.;
参考文献
Femec, Douglas A.; Silver, Michael E.; Fay, Robert C.
Inorganic Chemistry, 1989 , vol. 28, p. 2789 - 2796
参考文献
Nachmias
Annales de Chimie (Cachan, France), 1952 , vol. <12> 7, p. 584,599
