二甲基二硫代氨基甲酸钠合成路线 （共 123 条）
反应条件
2-methyl-butane; water
参考文献
Phillips Petr.Co.
Patent: US2792394 , 1954 ;
反应条件
in acetone soln. of (C4H9)2SnCl2 in acetone added dropwise with stirring to soln. of organic compound in acetone, mixture allowed to stand at room temp. for 1 h; filtered, solvent removed from filtrate, residue recrystd. from Et2O, elem. anal.;
参考文献
Sharma, C. P.; Kumar, N.; Khandpal, M. C.; Chandra, S.; Bhide, V. G.
Journal of Inorganic and Nuclear Chemistry, 1981 , vol. 43, p. 923 - 930
反应条件
in ethanol 18 h; Ambient temperature;
参考文献
Ishida, Masaru; Ichikawa, Kiyoshi; Asano, Masahiko; Nakanishi, Hirofumi; Kato, Shinzi
Synthesis, 1987 , # 4 p. 349 - 353
反应条件
N,N-dimethylaminoacetic acid; copper(l) iodide in N,N-dimethyl-formamide T=110°C; Ullmann-type coupling; 22 h;
参考文献
Liu, Yunyun; Bao, Weiliang
Tetrahedron Letters, 2007 , vol. 48, # 27 p. 4785 - 4788
反应条件
1: toluene With polymer-supported phenyliodine(III) diacetate; sulfuric acid in acetic acid T=20°C; Arylation; 20 h; 2: N,N-dimethyldithiocarbamic acid sodium salt in N,N-dimethyl-formamide T=60 - 70°C; Condensation; 12 h;
参考文献
Chen
Journal of Chemical Research - Part S, 2000 , # 7 p. 352 - 353
反应条件
in tert-butyl alcohol T=70°C; 10 h;
参考文献
Chen, Zhen-Chu; Jin, You-Yuan; Stang, Peter J.
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4117 - 4118
参考文献
Kulka
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1093,1099
反应条件
N,N-dimethylaminoacetic acid; copper(l) iodide in N,N-dimethyl-formamide T=110°C; Ullmann-type coupling; 22 h;
参考文献
Liu, Yunyun; Bao, Weiliang
Tetrahedron Letters, 2007 , vol. 48, # 27 p. 4785 - 4788
反应条件
in tert-butyl alcohol T=70°C; 5 h;
参考文献
Chen, Zhen-Chu; Jin, You-Yuan; Stang, Peter J.
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4117 - 4118
反应条件
1: benzene With polymer-supported phenyliodine(III) diacetate; sulfuric acid in acetic acid T=20°C; Arylation; 60 h; 2: N,N-dimethyldithiocarbamic acid sodium salt in N,N-dimethyl-formamide T=60 - 70°C; Condensation; 8 h;
参考文献
Chen
Journal of Chemical Research - Part S, 2000 , # 7 p. 352 - 353
