2,6-二叔丁基-4-甲基苯酚合成路线 (共 290 条)
反应条件
potassium tert-butylate in N,N-dimethyl-formamide; Petroleum ether T=-60°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 21 p. 3696 - 3700
反应条件
C5CoN5O2(3-)*3C36H30NP2(1+) in dichloromethane T=-70°C; 0.0833333 h; starting material added in dimer form; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 21, p. 3407 - 3408
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; chlorobenzene T=120°C; 4 h;
参考文献
Baik, Woonphil; Lee, Hyun Joo; Koo, Sangho; Kim, Byeong Hyo
Tetrahedron Letters, 1998 , vol. 39, # 44 p. 8125 - 8128
参考文献
Journal of Organic Chemistry, , vol. 56, # 3 p. 921 - 927
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=25°C; 24 h; Yield given;
参考文献
Chemistry Letters, , # 5 p. 961 - 964
反应条件
in triethylamine Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 3 p. 921 - 927
反应条件
1: pyridine / petroleum ether / 1.) 30 min, 0 deg C, 2.) 2 h, room temp. 2: 54 percent Spectr. / t-BuOK / petroleum ether; dimethylformamide / 2 h / -60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 21 p. 3696 - 3700
反应条件
T=70°C; Friedel-Crafts alkylation; 8 h; Ionic liquidAutoclave; Kinetics; ConcentrationReagent/catalystTemperatureTime; regioselective reaction;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 321, # 1-2 p. 34 - 41
反应条件
oxygen; ozone in water 0.25 - 2 h;
参考文献
US2008/242875 A1, ;
Page/Page column 5-8; 15-16 ;
反应条件
Cu0.5Co0.5Fe2O4 in nitromethane T=100°C; 6.5 h;
参考文献
Journal of Chemical Sciences, , vol. 124, # 4 p. 827 - 834