2,6-二叔丁基-4-甲基苯酚合成路线 （共 290 条）
反应条件
potassium hydroxide; iodine in methanol
other bases, other solvent; Product distribution;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3046 - 3050
反应条件
sodium methylate in methanol
Ambient temperatureelectrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.1 M NaClO4; 0.5 V; effect of the electricity consumption; Product distributionMechanism;
参考文献
Ohmori, Hidenobu; Ueda, Chihiro; Tokuno, Yoshimi; Maeda, Hatsuo; Masui, Masaichiro
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 9 p. 4007 - 4011
反应条件
zinc(II) chloride; trichlorophosphate
参考文献
Kosolapoff,G.M. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , vol. <C>, p. 815 - 818
反应条件
1: PhI(OAc)2 / CH2Cl2 / 2.5 h / 20 °C
2: 14 percent / Dess Martin periodinane / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Liu, Qin; Rovis, Tomislav
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 598 - 604
反应条件
perchloric acid; lead dioxide
0.133333 h;
参考文献
Omura, Kanji
Synthesis, 2010 , # 2 art. no. F17409SS, p. 208 - 210
反应条件
triethylamine in dichloromethane
T=0 - 20°C;
参考文献
Gillard, John W.; Fortin, Rejean; Morton, Howard E.; Yoakim, Christiane; Quesnelle, Claude A.; at al.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2602 - 2608
反应条件
pyridine in isobutyramide; water
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: US2011/193019 A1, 2011 ;
反应条件
1: 93 percent / NBS; DMSO
2: p-toluenesulfonic acid / benzene / 48 h / Heating
3: K2CO3 / 18-crown-6 / acetone; dimethylformamide / 48 h / Heating
4: HCl / acetone / 40 °C
5: KBH4; MeOH / tetrahydrofuran / 24 h / 50 °C
View Scheme
参考文献
Shanahan, Charles S.; McGrath, Dominic V.
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 1054 - 1056
反应条件
N-bromosuccinmide; diethylaluminium chloride in dimethyl sulfoxide
Cycloaddition; Diels-Alder reaction; 7 h; Heating;
参考文献
Baik, Woonphil; Lee, Hyun Joo; Jang, Jung Min; Koo, Sangho; Kim, Byeong Hyo
Journal of Organic Chemistry, 2000 , vol. 65, # 1 p. 108 - 115
反应条件
in hexane; methyl acetate; water
参考文献
Schering Aktiengesellschaft
Patent: US5523428 A1, 1996 ;
