N,N'-二苯基-3,4,9,10-二甲酰亚胺合成路线 （共 8 条）
反应条件
2,6-dichloro-benzonitrile; potassium tert-butylate in acetonitrile
T=170°C;
参考文献
Sakamoto; Pac
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 94 - 98
参考文献
Maki; Hashimoto
Kogyo Kagaku Zasshi, 1951 , vol. 54, p. 544
Chem.Abstr., 1953 , p. 6413
Full Text Show Details
I.G. Farbenind.
Patent: DE636891 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 23, p. 1128
反应条件
1: With [2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl-formamide
T=70°C; 6 h;
2: With dihydrogen peroxide in N,N-dimethyl-formamide
T=30 - 40°C; 0.5 h;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 6 p. 861 - 865
反应条件
2: 47 percent / t-BuOK; DBN / acetonitrile / 170 °C
View Scheme
参考文献
Sakamoto; Pac
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 94 - 98
反应条件
1: With 1,10-phenanthroline; nickel dichloride; zinc in N,N-dimethyl-formamide
T=70°C; 6 h;
2: With dihydrogen peroxide in N,N-dimethyl-formamide
T=30 - 40°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 6 p. 861 - 865
参考文献
Kalle and Co.
Patent: DE386057 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 485
反应条件
elctrochemical reduction; Product distributionMechanism;
参考文献
Vorozhtsov, G.N.; Ryabinin, V.A.; Starichenko, V.F.; Shein, S.M.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 887 - 894
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1024 - 1033
反应条件
cathodic reduction; Product distributionMechanism;
参考文献
Vorozhtsov, G.N.; Ryabinin, V.A.; Starichenko, V.F.; Shein, S.M.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 887 - 894
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1024 - 1033
