1,5-二羟基-4,8-二硝基蒽醌合成路线 （共 8 条）
反应条件
sulfuric acid; nitric acid T=10 - 15°C;
参考文献
DE89090 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 314
Chemische Berichte, , vol. 29, p. 2940
反应条件
sulfuric acid; sulfur trioxide; iodine; chlorine T=30°C;
参考文献
DyStar Textilfarben GmbH and Co. Deutschland KG
Patent: US2010/64452 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; palladium monocarbide in hydrogen
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4046785 A1, 1977 ;
参考文献
Schmidt,R.E.; Gattermann
Chemische Berichte, 1896 , vol. 29, p. 2940
反应条件
sodium sulfide; boric acid
1.) conc. H2SO4, -8 deg C, 1 h; 2.) aq. H2SO4, reflux, 4 h; 3.) water, ethanol, reflux, 2 h; Multistep reaction;
参考文献
Cognard; Hieu Phan; Basturk
Molecular crystals and liquid crystals, 1983 , vol. 91, # 3-4 p. 327 - 340
反应条件
sulfuric acid; sulfur trioxide; iodine; chlorine
T=30°C;
参考文献
DyStar Textilfarben GmbH and Co. Deutschland KG
Patent: US2010/64452 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
manganese(IV) dioxide; sodium chloride in Petroleum ether
参考文献
Merck Patent Gesellschaft mit beschrankter Haftung
Patent: US4532069 A1, 1985 ;
反应条件
sodium sulfide; boric acid
1.) conc. H2SO4, -8 deg C, 1 h; 2.) aq. H2SO4, reflux, 4 h; 3.) water, ethanol, reflux, 2 h; Multistep reaction;
参考文献
Cognard; Hieu Phan; Basturk
Molecular crystals and liquid crystals, 1983 , vol. 91, # 3-4 p. 327 - 340
