1,5-二甲酰基-4,8-二甲氧基萘合成路线 (共 7 条)
反应条件
aluminium trichloride in various solvent(s) T=0°C; 2 h;
参考文献
Tregub, N. G.; Knyazev, A. P.; Mezheritskii, V. V.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 143 - 146
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 168 - 172
反应条件
titanium tetrachloride in 1,2-dichloro-ethane
参考文献
Wipf, Peter; Jung, Jae-Kyu
Angewandte Chemie (International Edition in English), 1997 , vol. 36, # 7 p. 764 - 767
反应条件
aluminium trichloride in various solvent(s) T=0°C; 2 h;
参考文献
Tregub, N. G.; Knyazev, A. P.; Mezheritskii, V. V.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 143 - 146
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 168 - 172
反应条件
1: 45 percent / Br2 / CCl4 / 0.5 h / Heating 2: 1.) n-BuLi / 1.) THF, from -70 deg C to -65 deg C, 2.) THF, from -70 deg C to -60 deg C View Scheme
参考文献
Sylvester-Hvid; Sorensen; Schaumburg; Bechgaard; Christensen
Synthetic Communications, 1993 , vol. 23, # 13 p. 1905 - 1914
反应条件
toluene; trichlorophosphate Behandeln des Reaktionsgemisches mit wss.Natriumacetat;
参考文献
Buu-Hoi; Lavit
Journal of Organic Chemistry, 1955 , vol. 20, p. 1191,1195
反应条件
n-butyllithium 1.) THF, from -70 deg C to -65 deg C, 2.) THF, from -70 deg C to -60 deg C; Yield given. Multistep reaction;
参考文献
Sylvester-Hvid; Sorensen; Schaumburg; Bechgaard; Christensen
Synthetic Communications, 1993 , vol. 23, # 13 p. 1905 - 1914
反应条件
1: 1.) m-CPBA, 2.) LiOH 2: FeCl3 View Scheme
参考文献
Wipf, Peter; Jung, Jae-Kyu
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1092 - 1093