反应条件
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere 1.2: 1 h / -78 °C / Inert atmosphere 2.1: acetic acid; zinc / ethanol / 3 h / 0 °C / Inert atmosphere 3.1: diethylphosphoryl cyanide; triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere 4.1: LiAlH(Ot-Bu)3 / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere 5.1: pyridinium p-toluenesulfonate / 15 h / 0 °C / Inert atmosphere 6.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / -60 °C / Inert atmosphere 7.1: water; sodium hydroxide / propan-1-ol / Inert atmosphere; Reflux View Scheme
参考文献
Takita, Satoshi; Yokoshima, Satoshi; Fukuyama, Tohru
Synthesis, 2011 , # 23 art. no. H84011SS, p. 3848 - 3858
