2,6-双(2-吡啶基)-4(1H)-吡啶酮合成路线 （共 7 条）
反应条件
ammonium acetate in ethanol 6 h; Heating;
参考文献
Holbrey, John D.; Tiddy, Gordon J. T.; Bruce, Duncan W.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 11 p. 1769 - 1774
反应条件
potassium hydroxide; dibenzo-18-crown-6 in ethylene glycol dimethyl ether 48 h; Heating;
参考文献
Potts, Kevin T.; Konwar, Dilip
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4815 - 4816
反应条件
1: 75 percent / sodium hydride / tetrahydrofuran / 2 h / Heating 2: 75 percent / ammonium acetate / ethanol / Heating View Scheme
参考文献
Macromolecules, , vol. 39, # 24 p. 8207 - 8209
反应条件
1: 62 percent / PCl5, POCl3 / 12 h / Heating 2: 1.) <Ni(PPh3)2Cl2>, PPh3, Zn, NH4PF6, 2.) NaCN / 1.) DMF, room temp., 8h, 2.) MeCN, H2O, reflux, 1h View Scheme
参考文献
Constable, Edwin C.; Ward, Michael D.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , # 4 p. 1405 - 1409
反应条件
phosphorus pentachloride; trichlorophosphate 12 h; Heating;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , # 4 p. 1405 - 1409
反应条件
phosphorus pentabromide; phosphorus oxytribromide T=100°C; 12 h;
参考文献
The Trustees of the University of Pennsylvania
Patent: US7445845 B2, 2008 ;
Location in patent: Page/Page column 22-23; sheet 3 ;
反应条件
1: 2,2′:6′,2″-terpyridine-4′(1′H)-one With potassium carbonate in N,N-dimethyl-formamide
T=90°C; 0.5 h;
2: 1-n-heptylbromide in N,N-dimethyl-formamide
T=90°C; 20 h;
参考文献
Andres, Philip R.; Hofmeier, Harald; Lohmeijer, Bas G. G.; Schubert, Ulrich S.
Synthesis, 2003 , # 18 p. 2865 - 2871
