5-(苯基甲氧基)-2-戊烯酸乙酯合成路线 （共 9 条）
反应条件
in dichloromethane 5 h; Ambient temperature;
参考文献
Diez-Martin, David; Kotecha, Nikesh R.; Ley, Steven V.; Mantegani, Sergio; Menendez, J. Carlos; Organ, Helen M.; White, Andrew D.; Banks, Bernard J.
Tetrahedron, 1992 , vol. 48, # 37 p. 7899 - 7938
反应条件
1: (COCl)2; DMSO; Et3N / CH2Cl2 / 1.42 h / -50 - 20 °C 2: 11.28 g / CH2Cl2 View Scheme
参考文献
Lin, Shuangzheng; Deiana, Luca; Tseggai, Abrehet; Cordova, Armando
European Journal of Organic Chemistry, 2012 , # 2 p. 398 - 408
反应条件
1: 91 percent / NaH; tetra-n-butylammonium iodide / tetrahydrofuran / 20 °C 2: (COCl)2; DMSO; Et3N / CH2Cl2 / 1.42 h / -50 - 20 °C 3: 11.28 g / CH2Cl2 View Scheme
参考文献
Lin, Shuangzheng; Deiana, Luca; Tseggai, Abrehet; Cordova, Armando
European Journal of Organic Chemistry, 2012 , # 2 p. 398 - 408
反应条件
1: 89 percent / 1.)diisobutylaluminum hydride, 2.)methanol / toluene / Ambient temperature 2: oxalyl chloride - DMSO, Et3N / CH2Cl2 / 0.75 h / -70 - -65 °C 3: 181.2 g / CH2Cl2 / 1.)-70 -> -65 deg C, 15 min., 2.)r.t., 4 h View Scheme
参考文献
Martinelli, Michael J.
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5065 - 5073
反应条件
1: p-toluenesulfonic acid monohydrate / toluene / 2.5 h / Heating 2: 89 percent / 1.)diisobutylaluminum hydride, 2.)methanol / toluene / Ambient temperature 3: oxalyl chloride - DMSO, Et3N / CH2Cl2 / 0.75 h / -70 - -65 °C 4: 181.2 g / CH2Cl2 / 1.)-70 -> -65 deg C, 15 min., 2.)r.t., 4 h View Scheme
参考文献
Martinelli, Michael J.
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5065 - 5073
反应条件
1.1: O3 / CH2Cl2 / -78 °C 1.2: 86 percent / Ph3P 2.1: CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Hon, Yung-Son; Lu, Ling; Chang, Rong-Chi; Lin, Sheng-Wun; Sun, Pei-Pei; Lee, Chia-Fu
Tetrahedron, 2000 , vol. 56, # 47 p. 9269 - 9279
反应条件
in benzene 46 h; Heating; Yield given. Yields of byproduct given;
参考文献
Hon, Yung-Son; Lu, Ling; Chang, Rong-Chi; Lin, Sheng-Wun; Sun, Pei-Pei; Lee, Chia-Fu
Tetrahedron, 2000 , vol. 56, # 47 p. 9269 - 9279
反应条件
in dichloromethane T=-78 - 20°C; Wittig type reaction;
参考文献
Hon, Yung-Son; Lu, Ling; Chang, Rong-Chi; Lin, Sheng-Wun; Sun, Pei-Pei; Lee, Chia-Fu
Tetrahedron, 2000 , vol. 56, # 47 p. 9269 - 9279
参考文献
Nakada, Masahisa; Kobayashi, Susumu; Ohno, Masaji; Iwasaki, Shigeo; Okuda, Shigenobu
Tetrahedron Letters, 1988 , vol. 29, # 32 p. 3951 - 3954
