2-(5-乙酰氧基-4,6,7-三甲基-2,3-二氢苯并呋喃-2-基)乙酸合成路线 (共 2 条)
反应条件
1: ZnCl2 / heptane / 2 h / Heating 2: 1.) 20percent aq. KOH, sodium hydrosulfite, 2.) conc. H2SO4 / 1.) reflux, 2.5 h, 2.) 80 deg C, 4 h View Scheme
参考文献
Ceccarelli; De Vellis; Scuri; Zanarella
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 3 p. 679 - 690
反应条件
potassium hydroxide; sodium disulfite; sulfuric acid 1.) reflux, 2.5 h, 2.) 80 deg C, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ceccarelli; De Vellis; Scuri; Zanarella
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 3 p. 679 - 690