2-氯-7-甲氧基喹啉-3-甲腈合成路线 (共 5 条)
反应条件
ammonia; iodine in tetrahydrofuran; water T=20°C; 1.41667 h;
参考文献
Upadhyay, Shraddha; Chandra, Atish; Singh, Radhey M.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 1 p. 152 - 154
反应条件
trichlorophosphate in 1,2-dichloro-ethane; N,N-dimethyl-formamide 20 h; Ambient temperature;
参考文献
Adams, David R.; Adams, Chitra
Synthetic Communications, 1990 , vol. 20, # 3 p. 469 - 475
反应条件
1: 95 percent / triethyl ortoformate, TsOH / 20 h / 120 °C 2: 77 percent / POCl3 / 1,2-dichloro-ethane; dimethylformamide / 20 h / Ambient temperature View Scheme
参考文献
Adams, David R.; Adams, Chitra
Synthetic Communications, 1990 , vol. 20, # 3 p. 469 - 475
反应条件
1: H2O 2: 89 percent / POCl3 / 80 - 90 °C 3: 75 percent / aq. ammonia; cerium(IV) ammonium nitrate / 0 °C View Scheme
参考文献
Srivastava, Ambika; Singh, Mrityunjay K.; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 292 - 296
反应条件
1: 89 percent / POCl3 / 80 - 90 °C 2: 75 percent / aq. ammonia; cerium(IV) ammonium nitrate / 0 °C View Scheme
参考文献
Srivastava, Ambika; Singh, Mrityunjay K.; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 1 p. 292 - 296