反应条件
1: 1.) t-BuLi, 2.) O2 / 1.) THF, -78 deg C 2: PCC/Al2O3 3: i-Pr2NEt, DMAP / CH2Cl2 4: 1.) NaN(TMS)2 / 1.) THF, HMPA 5: pyridine*(HF)x / tetrahydrofuran 6: 83 percent / n-Bu4NF 7: 49 percent / 3 N HCl / tetrahydrofuran View Scheme
参考文献
Smith, Amos B.; Noda, Ichio; Remiszewski, Stacy W.; Liverton, Nigel J.; Zibuck, Regina
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 3977 - 3979
