4-甲酰基苯硼酸频哪醇酯合成路线 （共 30 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium acetate in 1,4-dioxane T=80°C; 15 h; Inert atmosphere;
参考文献
ACHAOGEN, INC.; PATTERSON, Brian D.; LU, Qing; AGGEN, James Bradley; DOZZO, Paola; KASAR, Ramesh Annasaheb; LINSELL, Martin Sheringham; KANE, Timothy Robert; GLIEDT, Micah James; HILDEBRANDT, Darin James; MCENROE, Glenn A.; COHEN, Frederick
Patent: WO2013/170165 A1, 2013 ;
Location in patent: Page/Page column 93 ;
反应条件
in tetrahydrofuran; toluene
参考文献
Shema-Mizrachi, Meital; Aharoni, Anna; Iliashevsky, Olga; Lemcoff
Israel Journal of Chemistry, 2009 , vol. 49, # 1 p. 1 - 8
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium acetate in 1,4-dioxane T=110°C; 2 h; Inert atmosphere;
参考文献
Chow, Wing Kin; Yuen, On Ying; So, Chau Ming; Wong, Wing Tak; Kwong, Fuk Yee
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3543 - 3548
反应条件
n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane T=-60°C;
参考文献
Browne, Duncan L.; Baumann, Marcus; Harji, Bashir H.; Baxendale, Ian R.; Ley, Steven V.
Organic Letters, 2011 , vol. 13, # 13 p. 3312 - 3315
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in dimethyl sulfoxide T=80°C; 2 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
1: C7H5BrMgO With boric acid trimethyl ester in tetrahydrofuran T=-78 - 25°C; 2: 2,3-dimethylbutane-2,3-diol With acetic acid in tetrahydrofuran T=20°C; 4 h;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
1: p-bromophenyl bromide; 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 0.5 h; 2: With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 0.333333 h; 3: N,N-dimethyl-formamide in tetrahydrofuran; pentane T=-78 - 20°C; 1 h; Further stages.;
参考文献
Jiang, Qin; Ryan, Meagan; Zhichkin, Paul
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6618 - 6620
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 6 h; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 6913 - 6917
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-60°C; Flow reactor;
参考文献
Newby, James A.; Huck, Lena; Blaylock, D. Wayne; Witt, Paul M.; Ley, Steven V.; Browne, Duncan L.
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 263 - 271
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 17 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
