4-甲酰基苯硼酸频哪醇酯合成路线 （共 30 条）
反应条件
tert.-butylnitrite in acetonitrile T=80°C; 2 h;
参考文献
Qiu, Di; Jin, Liang; Zheng, Zhitong; Meng, He; Mo, Fanyang; Wang, Xi; Zhang, Yan; Wang, Jianbo
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1923 - 1933
反应条件
potassium tetrachloropalladate; potassium acetate T=70°C; Miyaura borylation; 2.5 h; Inert atmosphere;
参考文献
Bej, Ansuman; Srimani, Dipankar; Sarkar, Amitabha
Green Chemistry, 2012 , vol. 14, # 3 p. 661 - 667
反应条件
1: triethylamine / dichloromethane 2: potassium acetate / tert-butyl alcohol / 6 h / 90 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; tetrakis(triphenylphosphine) palladium(0) Suzuki cross-coupling; Heating;
参考文献
Synthetic Communications, , vol. 37, # 5 p. 667 - 674
反应条件
potassium fluoride in N,N-dimethyl-formamide T=50°C; 18 h; Inert atmosphere;
参考文献
Litvinas, Nichole D.; Fier, Patrick S.; Hartwig, John F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 536 - 539
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene Inert atmosphereReflux;
参考文献
PROZYMEX A/S; PEDERSEN, John; LAURITZEN, Conni
Patent: WO2012/130299 A1, 2012 ;
Location in patent: Page/Page column 113 ;
WO 2012/130299 A1
反应条件
1-fluoro-2,4,6-trimethylpyridinium hexafluorophosphate; C10H18CuN2(1+)*CF3O3S(1-); silver fluoride in tetrahydrofuran T=50°C; 18 h; Inert atmosphere;
参考文献
Fier, Patrick S.; Luo, Jingwei; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 7 p. 2552 - 2559
反应条件
hydroxylamine hydrochloride; 1-propanephosphonic acid cyclic anhydride; triethylamine in ethyl acetate; N,N-dimethyl-formamide T=100°C;
参考文献
Synlett, , # 20 p. 3378 - 3382
反应条件
potassium tetrachloropalladate; cesium fluoride T=70°C; Suzuki coupling; 3 h; Inert atmosphere;
参考文献
Green Chemistry, , vol. 14, # 3 p. 661 - 667
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) Suzuki cross-coupling; Heating;
参考文献
Miura, Masanori; Koike, Takanori; Ishihara, Tsukasa; Sakamoto, Shuichi; Okada, Minoru; Ohta, Mitsuaki; Tsukamoto, Shin-Ichi
Synthetic Communications, 2007 , vol. 37, # 5 p. 667 - 674
