4-甲酰基苯硼酸频哪醇酯合成路线 （共 30 条）
反应条件
C92H36BF2N3O; N-ethyl-N,N-diisopropylamine in dichloromethane; acetonitrile 4 h; IrradiationInert atmosphere; Reagent/catalystTime;
参考文献
Chemistry - A European Journal, , vol. 19, # 51 p. 17472 - 17482
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene T=20°C; Inert atmosphereReflux;
参考文献
PROZYMEX A/S; PEDERSEN, John; LAURITZEN, Conni
Patent: WO2012/130299 A1, 2012 ;
Location in patent: Page/Page column 109 ;
WO 2012/130299 A1
反应条件
potassium carbonate in tetrahydrofuran; methanol T=40°C;
参考文献
Synlett, , # 19 p. 3037 - 3041
反应条件
1.1: 80 percent / NaBH4 / methanol / 0.17 h / 4 °C 2.1: Et3N; MsCl / CH2Cl2 / 1 h / 4 °C 2.2: 88 percent / LiBr / acetone / Heating View Scheme
参考文献
De Filippis, Arnault; Morin, Christophe; Thimon, Christian
Synthetic Communications, 2002 , vol. 32, # 17 p. 2669 - 2676
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran; water 48 h; RefluxInert atmosphere;
参考文献
Journal of Materials Chemistry, , vol. 21, # 14 p. 5451 - 5456
反应条件
1: sodium tetrahydroborate / 5 h / 20 °C 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C 4: hydrazine hydrate / tetrahydrofuran / 12 h / |Reflux View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: sodium tetrahydroborate / 5 h / 20 °C 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C / |Inert atmosphere 3: potassium carbonate / N,N-dimethyl-formamide / 72 h / 20 °C View Scheme
参考文献
Chung, Sheng-Hsuan; Lin, Ting-Ju; Hu, Qian-Yu; Tsai, Chia-Hua; Pan, Po-Shen
Molecules, 2013 , vol. 18, # 10 p. 12346 - 12367
反应条件
palladium diacetate; triphenylphosphine; p-benozquinone T=20°C; P=760.051 Torr; 5 h;
参考文献
Yamamoto, Yoshihiko
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 2-3 p. 478 - 492
反应条件
sodium tetrahydroborate in methanol T=4°C; 0.166667 h;
参考文献
De Filippis, Arnault; Morin, Christophe; Thimon, Christian
Synthetic Communications, 2002 , vol. 32, # 17 p. 2669 - 2676
反应条件
trimethylsilylazide; tetrabutyl ammonium fluoride; copper(l) chloride in tetrahydrofuran; methanol
9 h; RefluxIn air;
参考文献
Li, Yu; Gao, Lian-Xun; Han, Fu-She
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 7969 - 7972
