in water; acetone 48 h; Ambient temperature;

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Multi-step reaction with 2 steps 1: 91 percent / K2CO3, copper, CuBr / dimethylformamide / 8 h / Heating2: 80 percent / 2 h / Heating  

Multi-step reaction with 5 steps 1: iron, acetic acid / 1 h / Heating2: acetic acid3: 92 percent / NaOCH3 / methanol / 24 h / Ambient temperature4: 91 percent / K2CO3, copper, CuBr / dimethylformamide / 8 h / Heating5: 80 percent / 2 h / Heating  

2 h;  Heating;