(间三联苯-5'-基)三甲基硅烷合成路线 (共 3 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; toluene 6 h; Heating;
参考文献
Miller, Timothy M.; Neenan, Thomas X.; Zayas, Roberto; Bair, Harvey E.
Journal of the American Chemical Society, 1992 , vol. 114, # 3 p. 1018 - 1025
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: 79 percent / tetrahydrofuran; hexane / -78 - 20 °C 2.1: 80 percent / Pd(PPh3)4; aq. K2CO3 / tetrahydrofuran / 24 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 7 p. 2358 - 2367
反应条件
1: BBr3 2: aq. KOH View Scheme
参考文献
Gong; Hu; Pu
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2358 - 2367