(S)-(+)-1,1'-联-2-萘酚二(三氟甲磺酸酯)合成路线 (共 10 条)
反应条件
pyridine in dichloromethane T=0°C; 6 h;
参考文献
Uozumi, Yasuhiro; Tanahashi, Asako; Lee, Sang-Yong; Hayashi, Tamio
Journal of Organic Chemistry, 1993 , vol. 58, # 7 p. 1945 - 1948
反应条件
4-(N,N-dimethlyamino)pyridine; trifluoromethanesulfonic acid anhydride in dichloromethane
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.; Takasago International Corporation
Patent: EP614870 A2, 1994 ;
反应条件
pyridine; hydrogenchloride in diethyl ether; hexane; dichloromethane; nitrogen
参考文献
Takasago International Corporation
Patent: US5824822 A1, 1998 ;
反应条件
triethylamine in dichloromethane T=-78 - 0°C; 2 h;
参考文献
Cao, Ziping; Liu, Yilin; Liu, Zhaoqun; Feng, Xiangqing; Zhuang, Minyang; Du, Haifeng
Organic Letters, 2011 , vol. 13, # 9 p. 2164 - 2167
反应条件
pyridine; trifluoromethylsulfonic anhydride in hexane; dichloromethane
参考文献
Takasago International Corporation
Patent: US5530150 A1, 1996 ;
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); zinc in N,N-dimethyl-formamide T=0 - 110°C; 48 h; Inert atmosphere;
参考文献
Liu, Lei; Wu, Hai-Chen; Yu, Jin-Quan
Chemistry - A European Journal, 2011 , vol. 17, # 39 p. 10828 - 10831