反应条件
1.1: sodium tetrahydroborate / methanol / 1.5 h / 0 - 10 °C 2.1: methanol; water / 1 h / 0 - 20 °C 2.2: 2 h / 0 - 20 °C 3.1: hydrogenchloride / water / 24 h / 20 °C 4.1: sodium tetrahydroborate; trifluoroacetic acid / dichloromethane / 25 h / 0 - 20 °C 5.1: iodine; potassium acetate / ethanol / 3 h / 80 °C View Scheme
参考文献
Mao, Yongjun; Song, Shuai; Zhao, Dongmei; Cheng, Maosheng
Heterocycles, 2013 , vol. 87, # 12 p. 2633 - 2640