二甲基-3,3’-联砒啶-5,5’-二羧酸合成路线 (共 2 条)
反应条件
1,1,1,2,2,2-hexabutyl-distannane; PhCH2Pd(PPh3)2Cl in N,N-dimethyl-formamide T=130°C; Stille coupling; 1 h;
参考文献
O'Neill, Brian T.; Yohannes, Daniel; Bundesmann, Mark W.; Arnold, Eric P.
Organic Letters, 2000 , vol. 2, # 26 p. 4201 - 4204
反应条件
NiBr2(PPh3)2; tetraethylammonium iodide; zinc in tetrahydrofuran T=50°C; 20 h;
参考文献
Iyoda; Otsuka; Sato; Nisato; Oda
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 1 p. 80 - 87