1H-苯并三唑-1-基氧三吡咯烷基六氟磷酸盐合成路线 (共 9 条)
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 178, # 2 p. 299 - 309
反应条件
hexafluorophosphate; trichlorophosphate Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 31, # 2 p. 205 - 208
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
参考文献
Reverse Proteomics Research Institute Co., Ltd.; Fujisawa Pharmaceutical Co., Ltd.
Patent: US2006/177943 A1, 2006 ;
反应条件
in tetrahydrofuran; dichloromethane T=20°C; 18 h;
参考文献
US2006/30583 A1, ;
Page/Page column 132-133 ;
US 20060030583 A1
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane 0.5 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2437 - 2446
反应条件
in diethyl ether; dichloromethane
参考文献
Oh, Jong Eun; Lee, Keon Hyoung; Park, Tae Gwan; Nam, Yoon Sung
Patent: US2004/13728 A1, 2004 ;
反应条件
1: diisopropylethylamine / CH2Cl2 / 0.5 h / Ambient temperature 2: 1.) POBr3, 2.) aq. KPF6 / 1.) CH3CN, r.t., 30 min View Scheme
参考文献
Coste, Jacques; Frerot, Eric; Jouin, Patrick
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2437 - 2446
反应条件
triethylamine in dichloromethane
参考文献
Bayer Aktiengesellschaft
Patent: US6562811 B1, 2003 ;
反应条件
in water; acetonitrile
T=20°C; Flow reactor;
参考文献
Nagaki, Aiichiro; Takahashi, Yusuke; Yoshida, Jun-Ichi
Chemistry - A European Journal, 2014 , vol. 20, # 26 p. 7931 - 7934