in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in ethylene glycol byproducts: PPh3, water; refluxed for 22 h (N2); short reflux condenser essential for the yields of CpRuCl(CO)PPh3 and ruthenocene; liquid distilled off up to 150-160°C; glycol phase extd. (benzene); exts. evapd.; sepd. on a column (silica gel, benzene); first fraction contained ruthenocene and CpRuH(CO)PPh3; second fraction evapd.; CpRuCl(CO)PPh3 washed (ethyl ether); dried;
参考文献
Journal of Organometallic Chemistry, , vol. 312, p. 349 - 356
in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
in dichloromethane (Ar); a soln. of ruthenium and iron complexes in CH2Cl2 was heated under reflux for 3 h; evapn.; column chromy. (SiO2, CH2Cl2 or CH2Cl2/ethyl acetate); recrystn.;
参考文献
Journal of Organometallic Chemistry, , vol. 610, # 1-2 p. 31 - 37
