反应条件
n-butyllithium in tetrahydrofuran; hexane addn. of n-Buli in hexane to soln. of org. compd. in THF (-78°C, N2 atmosphere, 1 h), addn. of B-compd., stirring (-78°C, 1.5 h); addn. of satd. soln. of aq. NH4Cl (-78°C), warming (room temp.),DDN: OF H2O, shaking with ether, washing of ether extracts (satd. aq. NaHCO3 and satd. brine), drying (Na2SO4), filtration, evapn. (vac.), crystn. (H2O);
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 715 - 720
