N-(4-苯基-1- 环己烯)-甲酰胺合成路线 (共 4 条)
反应条件
triphenylphosphine; methyloxirane in dichloromethane 18 h; Ambient temperature;
参考文献
Baldwin, J.E.; Aldous, D.J.; ONeil, I.A.
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2051 - 2054
反应条件
sulfuric acid in toluene Condensation; 12 h; HeatingDean-Stark-conditions;
参考文献
Maison, Wolfgang; Schlemminger, Imre; Westerhoff, Ole; Martens, Juergen
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 6 p. 1343 - 1360
反应条件
trifluoromethanesulfonic acid anhydride Dehydration;
参考文献
Lenoir, Isabelle; Smith, Marie L.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 5 p. 641 - 643
反应条件
trifluoromethylsulfonic anhydride; i-PrNEt; 3,3-dimethyldioxirane 1.) CH2Cl2, -40 deg C; 2.) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Baldwin, J. E.; ONeil, I. A.
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 2047 - 2050