4-[3-(三氟甲基)-3H-双吖丙啶-3-基]苯甲醛合成路线 （共 6 条）
反应条件
titanium tetrachloride in various solvent(s) T=20°C; 1 h;
参考文献
Nakashima, Hiroyuki; Hashimoto, Makoto; Sadakane, Yutaka; Tomohiro, Takenori; Hatanaka, Yasumaru
Journal of the American Chemical Society, 2006 , vol. 128, # 47 p. 15092 - 15093
反应条件
Amberlyst 15 in acetone Ambient temperature;
参考文献
Delfino, Jose M.; Schreiber, Stuart L.; Richards, Frederic M.
Journal of the American Chemical Society, 1993 , vol. 115, # 9 p. 3458 - 3474
反应条件
sodium hydrogencarbonate; dimethyl sulfoxide T=100°C; 10 h;
参考文献
Resek; Bhattacharya; Khorana
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7598 - 7601
反应条件
1: 73 percent / triethylamine (TEA), iodine / methanol / 1 h 2: 100 percent / Amberlyst 15 / acetone / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 9 p. 3458 - 3474
反应条件
sodium tetrahydroborate in ethanol T=20°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 128, # 47 p. 15092 - 15093
反应条件
1: 100 percent / NaBH4 / ethanol / 4 h / 20 °C
2: 100 percent / CBr4; Ph3P / CH2Cl2 / 4 h / 20 °C
View Scheme
参考文献
Nakashima, Hiroyuki; Hashimoto, Makoto; Sadakane, Yutaka; Tomohiro, Takenori; Hatanaka, Yasumaru
Journal of the American Chemical Society, 2006 , vol. 128, # 47 p. 15092 - 15093
