4-[2-(2-甲基氨基丙基)苯基]硫基苯-1,2-二醇合成路线 （共 7 条）
反应条件
boron tribromide in chloroform 5 h; Ambient temperature;
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: 70 percent / Na2CO3 / hexamethylphosphoric acid triamide / 3.5 h / 100 °C 2: 4.8 g / butylamine / acetic acid / 5 h / Heating 3: LiAlH4 / diethyl ether / 2 h 4: 16.2 g / 150 °C 5: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 6: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: 4.8 g / butylamine / acetic acid / 5 h / Heating 2: LiAlH4 / diethyl ether / 2 h 3: 16.2 g / 150 °C 4: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 5: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: LiAlH4 / diethyl ether / 2 h 2: 16.2 g / 150 °C 3: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 4: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 2: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: 16.2 g / 150 °C 2: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 3: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
反应条件
1: 70 percent / Na2CO3 / hexamethylphosphoric acid triamide / 3.5 h / 100 °C 2: 4.8 g / butylamine / acetic acid / 5 h / Heating 3: LiAlH4 / diethyl ether / 2 h 4: 16.2 g / 150 °C 5: LiAlH4 / benzene; diethyl ether / 5.5 h / Heating 6: BBr3 / CHCl3 / 5 h / Ambient temperature View Scheme
参考文献
Urban, Jiri; Sedivy, Zdenek; Holubek, Jiri; Svatek, Emil; Ryska, Miroslav; et al.
Collection of Czechoslovak Chemical Communications, 1990 , vol. 55, # 4 p. 1077 - 1098
