2,4,6-三硝基苯甲酸合成路线 （共 27 条）
参考文献
Sudborough
Journal of the Chemical Society, 1895 , vol. 67, p. 602
反应条件
ammonium hydroxide; ethanol
参考文献
Chem. Fabr. Griesheim
Patent: DE77353 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 34
参考文献
Desvergnes
Monit. scient., vol. <5> 16, p. 201
Chem. Zentralbl., 1926 , vol. 97, # II p. 3043
参考文献
Chem. Fabr. Griesheim
Patent: DE77353 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 34
参考文献
Chem. Fabr. Griesheim
Patent: DE77353 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 34
反应条件
hydrazine hydrate; iron(III) chloride in ethanol; water; acetic acid T=42 - 47°C; 4 h;
参考文献
Kislyi, Konstantine A.; Samet, Alexander V.; Strelenko, Yuri A.; Semenov, Victor V.
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2285 - 2291
反应条件
sodium hydroxide; titanium(III) ethylenediaminetetra-acetate T=20°C; 0.166667 h; 2,4-dinitrobenzoic acid, var. pH and reagents; Product distribution;
参考文献
Schmidt, Torsten C.; Steinbach, Klaus; Buetehorn, Ulf; Heck, Kerstin; Volkwein, Ute; Stork, Gottfried
Chemosphere, 1999 , vol. 38, # 13 p. 3119 - 3130
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 15, p. 87
反应条件
1: 90 percent / SOCl2 / dimethylformamide; 1,2-dichloro-ethane / 3 h / 20 - 70 °C 2: 61 percent / benzene / 5 h / 15 °C View Scheme
参考文献
Zlotin; Kislitsin; Samet; Serebryakov; Konyushkin; Semenov; Buchanan III; Gakh
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8430 - 8438
反应条件
1: 90 percent / SOCl2 / dimethylformamide; 1,2-dichloro-ethane / 3 h / 20 - 70 °C 2: 76 percent / H2O; benzene / 2 h / 5 - 6 °C 3: K2CO3 / dimethylformamide / 4 h / 15 °C View Scheme
参考文献
Zlotin; Kislitsin; Samet; Serebryakov; Konyushkin; Semenov; Buchanan III; Gakh
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8430 - 8438
