in benzene-d6 (Cp2Zr(H)Cl)x placed in an NMR tube and suspended with a soln. of Cp2Zr(Cl)CPh2OCH3 in benzene-d6; mixt. heated at 55°C for 7 h;; not isolated; reaction followed by NMR spectroscopy;;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2251
in tetrahydrofuran under N2 or Ar using Schlenk techniques; to macrocycle dry THF added; mixt. stirred rapidly for 1 h; GeCl4 added at room temp. dropwise with rapid stirring; allowed to stand for 24 h; filtered; washed (dry THF); dried (vac.); elem. anal.;
参考文献
Nitschke, Jonathan R.; Don Tilley
Journal of Organometallic Chemistry, 2003 , vol. 666, # 1-2 p. 15 - 22
