methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
methylaluminoxane in benzene-d6 under Ar, standard Schlenk techniques; solid dichloride Zr complex mixedwith 1 equiv. of Cp2ZrClMe; dissolved in benzene-d6; a minute amt. of s olid methylaluminoxane added; equil. reached within several min; not isolated; monitored by (1)H NMR spectra;
