2,5-脱水-3,4-二苄基-D-山梨糖醇合成路线 （共 12 条）
反应条件
ammonium formate in methanol T=90°C; 1 h; Microwave irradiation; Solvent; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 54, # 9 p. 1087 - 1089
反应条件
osmium(VIII) oxide; trimethylamine-N-oxide; camphor-10-sulfonic acid in dichloromethane
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 8 p. 948 - 951
反应条件
peracetic acid; sodium acetate; potassium bromide in acetic acid T=10°C; 2 h;
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: pyridinium p-toluenesylfonate / acetone 2: NaH / tetrahydrofuran / 0 °C 3: HgO, BF3*Et2O / tetrahydrofuran; H2O / 0.5 h 4: 7.0 g / diethyl ether / 2 h / 0 °C 5: 86 percent / AcOH / H2O / 16 h 6: H2SO4 / tetrahydrofuran / 50 °C 7: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: NaH / tetrahydrofuran / 0 °C 2: HgO, BF3*Et2O / tetrahydrofuran; H2O / 0.5 h 3: 7.0 g / diethyl ether / 2 h / 0 °C 4: 86 percent / AcOH / H2O / 16 h 5: H2SO4 / tetrahydrofuran / 50 °C 6: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: 7.0 g / diethyl ether / 2 h / 0 °C 2: 86 percent / AcOH / H2O / 16 h 3: H2SO4 / tetrahydrofuran / 50 °C 4: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: HgO, BF3*Et2O / tetrahydrofuran; H2O / 0.5 h 2: 7.0 g / diethyl ether / 2 h / 0 °C 3: 86 percent / AcOH / H2O / 16 h 4: H2SO4 / tetrahydrofuran / 50 °C 5: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: H2SO4 / tetrahydrofuran / 50 °C 2: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: 86 percent / AcOH / H2O / 16 h 2: H2SO4 / tetrahydrofuran / 50 °C 3: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
反应条件
1: NaH / tetrahydrofuran / 0 °C 2: HgO, BF3*Et2O / tetrahydrofuran; H2O / 0.5 h 3: 7.0 g / diethyl ether / 2 h / 0 °C 4: 86 percent / AcOH / H2O / 16 h 5: H2SO4 / tetrahydrofuran / 50 °C 6: 81 percent / KBr, AcO2H, NaOAc / acetic acid / 2 h / 10 °C View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 18, # 2 p. 165 - 190
