1292766-17-6合成路线 (共 12 条)
参考文献
Higashino, Tomohiro; Rodriguez-Morgade, M. Salome; Osuka, Atsuhiro; Torres, Tomas
Chemistry - A European Journal, 2013 , vol. 19, # 31 p. 10353 - 10359
反应条件
bis-triphenylphosphine-palladium(II) chloride; silver benzoate in tetrahydrofuran T=65°C; 24 h; Inert atmosphere;
参考文献
Maltsev, Oleg V.; Poethig, Alexander; Hintermann, Lukas
Organic Letters, 2014 , vol. 16, # 5 p. 1282 - 1285
反应条件
palladium diacetate; triphenylphosphine in acetonitrile T=130°C; 0.5 h; Inert atmosphereMicrowave irradiation; Temperature;
参考文献
Maltsev, Oleg V.; Poethig, Alexander; Hintermann, Lukas
Organic Letters, 2014 , vol. 16, # 5 p. 1282 - 1285
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of PhCOSCH2CONMe2 (1 equiv.) with CH3OC6H4B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of PhCOSCH2CONMe2 (1 equiv.) with (2-naphthyl)B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in acetic acid addn. of C4H3SCOOCu (1.6 eqiuv.) to the reaction of PhCOSCH2CONMe2 (1 equiv.) with (C10H7)B(OH)2 (1 equiv.) in acetic acid in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of PhCOSCH2CONMe2 (1 equiv.) with (CH3OC6H4)B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of CF3COSC6H4CH3 (1 equiv.) with (NO2C6H4)B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of HOC6H4COSC2H5 (1 equiv.) with PhB(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
反应条件
Pd2(dba)3*CHCl3/tris(2-furyl)phosphine in tetrahydrofuran
addn. of 1.6 equiv. of C4H3SCOOCu to the reaction of C3H4N2COSC6H5 (1 equiv.) with (C6H5CHCH)B(OH)2 (1 equiv.) in THF in presence of 1percent Pd2(dba)3*CHCl3/(tris-2-furylphosphine), holding for 18 h at 50°C;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261