5-异丙基-6-甲基-2-(2-甲基-2-丙基)-1,3-二恶烷-4-酮合成路线 (共 2 条)
反应条件
1-tert-butyl-4,4,4-tris(dimethylamino)-2,2-bis[tris(dimethylamino)-phosphoranylidenamino]-2Λ54Λ5-catenadi(phosphazene) in tetrahydrofuran T=-95°C; 1 h; Yields of byproduct given;
参考文献
Pietzonka, Thomas; Seebach, Dieter
Chemische Berichte, 1991 , vol. 124, # 8 p. 1837 - 1843
反应条件
copper(l) iodide; boron trifluoride diethyl etherate 1.) ether, -20 deg C, 20 min, 2.a) -78 deg C, 1 h up to -40 deg C, 1 h, b) 6 h; Yield given. Multistep reaction;
参考文献
Amberg, Willi; Seebach, Dieter
Chemische Berichte, 1990 , vol. 123, # 12 p. 2413 - 2428