1: hydrogenchloride; palladium 10 on activated carbon; hydrogen / ethanol; isopropyl alcohol / 6 h / 20 °C / |Schlenk technique 2: HATU; triethylamine / acetonitrile; dichloromethane / |Cooling with ice; |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Kolmakov, Kirill; Wurm, Christian A.; Hennig, Rene; Rapp, Erdmann; Jakobs, Stefan; Belov, Vladimir N.; Hell, Stefan W.
Chemistry - A European Journal, 2012 , vol. 18, # 41 p. 12986 - 12998