1: With benzotriazol-1-ol; N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide 15 h; 2: With hydrogen; 5-palladium/activated carbon in ethanol T=200°C; 5.08333 h;
hydrogen; palladium on activated charcoal in ethanol P=3040 Torr; 18 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 5 p. 1328 - 1337