(9ci)-n,n,1-三甲基-1H-咪唑-2-羧酰胺合成路线 (共 2 条)
反应条件
in methanol; water 1) 0 deg C, 5 h; 2) room temperature, overnight;
参考文献
Bakhtiar, Cuross; Smith, Edward H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 239 - 244
反应条件
n-butyllithium 1) hexane, 2a) Et2O, -78 deg C, 2.4h, 2b) 0 deg C, 25 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ngochindo, Raphael I.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1645 - 1648