6-叠氮基-n-boc-己胺合成路线 （共 7 条）
反应条件
1: in dichloromethane T=20°C; 16 h; 2: With methanesulfonyl chloride; triethylamine in dichloromethane T=20°C; 16 h; 3: With sodium azide in DMF (N,N-dimethyl-formamide) T=100°C; 1 h;
参考文献
AUCKLAND UNISERVICES LIMITED; THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY
Patent: WO2004/26846 A1, 2004 ;
Location in patent: Page 53; 54 ;
反应条件
sodium azide; tetrabutylammomium bromide in water; toluene T=60°C; 3 h; Yield given;
参考文献
Synthesis, , p. 366 - 368
反应条件
1: 100 percent / CH2Cl2 / 12 h 2: triethylamine / toluene / 0.08 h / 0 °C 3: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C View Scheme
参考文献
Synthesis, , p. 366 - 368
反应条件
1: 100 percent / CH2Cl2 / 12 h 2: triethylamine / toluene / 0.08 h / 0 °C 3: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C View Scheme
参考文献
Synthesis, , p. 366 - 368
反应条件
1: triethylamine / toluene / 0.08 h / 0 °C 2: NaN3 / tetrabutylammonium bromide / toluene; H2O / 3 h / 60 °C View Scheme
参考文献
Synthesis, , p. 366 - 368
反应条件
chloroform; hydrogen; palladium on activated charcoal in methanol P=1551.4 Torr; 1 h;
参考文献
Mattingly, Phillip G.
Synthesis, 1990 , p. 366 - 368
反应条件
hydrogen; palladium on activated charcoal T=20°C; P=3102.97 Torr; 1 h;
参考文献
AUCKLAND UNISERVICES LIMITED; THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY
Patent: WO2004/26846 A1, 2004 ;
Location in patent: Page 54 ;
