5,5-二氟环己烷-1,3-二羧酸二甲酯合成路线 （共 3 条）
反应条件
diethylamino-sulfur trifluoride in ethanol; dichloromethane T=0 - 25°C; Inert atmosphere;
参考文献
H. LUNDBECK A/S
Patent: US2011/98299 A1, 2011 ;
Location in patent: Page/Page column 41 ;
反应条件
1: hydrogen; acetic acid / Rh/Al2O3 / methanol / 0 - 25 °C / 2844.39 Torr 2: triethylamine; pyridine-SO3 complex / dichloromethane; dimethyl sulfoxide / 10 - 25 °C / Inert atmosphere 3: diethylamino-sulfur trifluoride / dichloromethane; ethanol / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
H. LUNDBECK A/S
Patent: US2011/98299 A1, 2011 ;
反应条件
1: triethylamine; pyridine-SO3 complex / dichloromethane; dimethyl sulfoxide / 10 - 25 °C / Inert atmosphere 2: diethylamino-sulfur trifluoride / dichloromethane; ethanol / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
H. LUNDBECK A/S
Patent: US2011/98299 A1, 2011 ;
