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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1296306-77-8
合成路线
（共 5 条）
1296306-77-8
+
100-51-6
苯甲醇
→
反应条件
94569-19-4
+
87269-87-2
(1S,3S,5S)-2-氮杂双环[3,3,0]辛烷-3-羧酸苄酯盐酸盐
反应条件
thionyl chloride T=0 - 25°C; 13 h; Inert atmosphere;
参考文献
Kondaiah; Vivekanandareddy; Reddy, L. Amarnath; Anurkar, Smita V.; Gurav; Ravikumar; Bhattacharya, Apurba; Bandichhor, Rakeshwar
Synthetic Communications, 2011 , vol. 41, # 8 p. 1186 - 1191
1296306-77-8
→
反应条件
87269-87-2
(1S,3S,5S)-2-氮杂双环[3,3,0]辛烷-3-羧酸苄酯盐酸盐
反应条件
1.1: thionyl chloride / 13 h / 0 - 25 °C / Inert atmosphere 2.1: sodium hydroxide / water / pH 7.5 - 8 2.2: 0.5 h / 0 °C 2.3: 3 h / 25 °C 3.1: 5 Pd(II)/C(eggshell); hydrogen / ethanol; water / 3 h / 25 - 30 °C / 1838.93 - 2206.72 Torr / Autoclave 4.1: thionyl chloride / 13 h / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
Kondaiah; Vivekanandareddy; Reddy, L. Amarnath; Anurkar, Smita V.; Gurav; Ravikumar; Bhattacharya, Apurba; Bandichhor, Rakeshwar
Synthetic Communications, 2011 , vol. 41, # 8 p. 1186 - 1191
1296306-77-8
+
100-51-6
苯甲醇
→
反应条件
94569-19-4
+
87269-87-2
(1S,3S,5S)-2-氮杂双环[3,3,0]辛烷-3-羧酸苄酯盐酸盐
反应条件
thionyl chloride T=0 - 25°C; 13 h; Inert atmosphere;
参考文献
Kondaiah; Vivekanandareddy; Reddy, L. Amarnath; Anurkar, Smita V.; Gurav; Ravikumar; Bhattacharya, Apurba; Bandichhor, Rakeshwar
Synthetic Communications, 2011 , vol. 41, # 8 p. 1186 - 1191
1296306-77-8
→
反应条件
87269-87-2
(1S,3S,5S)-2-氮杂双环[3,3,0]辛烷-3-羧酸苄酯盐酸盐
反应条件
1.1: thionyl chloride / 13 h / 0 - 25 °C / Inert atmosphere 2.1: sodium hydroxide / water / pH 7.5 - 8 2.2: 0.5 h / 0 °C 2.3: 3 h / 25 °C 3.1: 5 Pd(II)/C(eggshell); hydrogen / ethanol; water / 3 h / 25 - 30 °C / 1838.93 - 2206.72 Torr / Autoclave 4.1: thionyl chloride / 13 h / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
Kondaiah; Vivekanandareddy; Reddy, L. Amarnath; Anurkar, Smita V.; Gurav; Ravikumar; Bhattacharya, Apurba; Bandichhor, Rakeshwar
Synthetic Communications, 2011 , vol. 41, # 8 p. 1186 - 1191
1296306-77-8
→
反应条件
109428-53-7
2-氮杂双环[3.3.0]辛烷-3-甲酸
反应条件
1.1: thionyl chloride / 13 h / 0 - 25 °C / Inert atmosphere 2.1: sodium hydroxide / water / pH 7.5 - 8 2.2: 0.5 h / 0 °C 2.3: 3 h / 25 °C 3.1: 5 Pd(II)/C(eggshell); hydrogen / ethanol; water / 3 h / 25 - 30 °C / 1838.93 - 2206.72 Torr / Autoclave View Scheme
参考文献
Kondaiah; Vivekanandareddy; Reddy, L. Amarnath; Anurkar, Smita V.; Gurav; Ravikumar; Bhattacharya, Apurba; Bandichhor, Rakeshwar
Synthetic Communications, 2011 , vol. 41, # 8 p. 1186 - 1191
