2-邻苯二甲酰亚胺基乳糖胺,七乙酸酯合成路线 （共 4 条）
反应条件
pyridine T=20 - 100°C; Acetylation; 4.2 h;
参考文献
Kretzschmar, Gerhard; Stahl, Wilhelm
Tetrahedron, 1998 , vol. 54, # 23 p. 6341 - 6358
反应条件
1.1: sodium methylate / methanol / pH 8 - 9 1.2: 26 h / 20 °C / Inert atmosphere 2.1: pyridine; 4-(N,N-dimethlyamino)pyridine / 18 h / 20 °C View Scheme
参考文献
Ohmae, Masashi; Takada, Junko; Murakami, Hiroaki; Kimura, -Shunsaku
Chemistry Letters, 2011 , vol. 40, # 5 p. 438 - 439
反应条件
1.1: 48 h / 40 °C 1.2: 20 °C 2.1: hydrogenchloride; Pearlman's catalist; hydrogen / water / 72 h / 20 °C / pH 1 3.1: sodium methylate / methanol / pH 8 - 9 3.2: 26 h / 20 °C / Inert atmosphere 4.1: pyridine; 4-(N,N-dimethlyamino)pyridine / 18 h / 20 °C View Scheme
参考文献
Ohmae, Masashi; Takada, Junko; Murakami, Hiroaki; Kimura, -Shunsaku
Chemistry Letters, 2011 , vol. 40, # 5 p. 438 - 439
反应条件
1.1: sodium methylate / methanol / pH 8 - 9 1.2: 26 h / 20 °C / Inert atmosphere 2.1: pyridine; 4-(N,N-dimethlyamino)pyridine / 18 h / 20 °C View Scheme
参考文献
Ohmae, Masashi; Takada, Junko; Murakami, Hiroaki; Kimura, -Shunsaku
Chemistry Letters, 2011 , vol. 40, # 5 p. 438 - 439
