5-甲酰基-3-甲基-4-异噁唑羧酸乙酯合成路线 （共 4 条）
反应条件
pyridinium chlorochromate in dichloromethane 72 h; Ambient temperature;
参考文献
Chantegrel, Bernard; Deshayes, Christian; Pujol, Bernard; Wei, Zhong Jia
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 927 - 934
反应条件
1: pyridine / diethyl ether / Ambient temperature 2: hydroxylamine hydrochloride, acetic acid / 0.5 h / Heating 3: 60 percent / pyridinium chlorochromate / CH2Cl2 / 72 h / Ambient temperature View Scheme
参考文献
Chantegrel, Bernard; Deshayes, Christian; Pujol, Bernard; Wei, Zhong Jia
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 927 - 934
反应条件
hydrazine hydrate in ethanol
T=20°C; 1 h;
参考文献
Cesari, Nicoletta; Biancalani, Claudio; Vergelli, Claudia; Dal Piaz, Vittorio; Graziano, Alessia; Biagini, Pierfrancesco; Ghelardini, Carla; Galeotti, Nicoletta; Giovannoni, Maria Paola
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7826 - 7835
反应条件
1: hydrazine hydrate / ethanol / 1 h / 20 °C
2: K2CO3 / dimethylformamide
View Scheme
参考文献
Cesari, Nicoletta; Biancalani, Claudio; Vergelli, Claudia; Dal Piaz, Vittorio; Graziano, Alessia; Biagini, Pierfrancesco; Ghelardini, Carla; Galeotti, Nicoletta; Giovannoni, Maria Paola
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7826 - 7835
