(OC-6-12)-(1,4,8,11,15,18,22,25-八丁氧基-29H,31H-酞菁根)二(三乙基硅醇)锗合成路线 （共 1 条）
反应条件
in pyridine; N,N-dimethyl-formamide; toluene Ar; GeCl4 added slowly (5 h) to refluxing cyanine in DMF; cooled; treated with CH2Cl2, dilute HCl and H2O; dried; evapd.; chromd. (Al2O3, CH2Cl2/MeOH, then toluene); Et3SiOH, pyridine and toluene added; refluxed for 2.5 h;; evapd.; chromy. (Bio-Beads S-X4, toluene); vacuum dried (75°C);;
参考文献
Journal of the American Chemical Society, , vol. 112, # 22 p. 8064 - 8070
