(6-邻苯二甲酰亚胺己基)三苯基溴化磷合成路线 （共 6 条）
反应条件
in toluene 15 h; Heating;
参考文献
Agathocleous, Demetrios C.; Bulman Page, Philip C.; Cosstick, Richard; Galpin, Ian J.; McLennan, Alexander G.; Prescott, Mark
Tetrahedron, 1990 , vol. 46, # 6 p. 2047 - 2058
反应条件
1: 80 percent / 0.25 h / 150 - 160 °C 2: 74.4 percent / CBr4/PPh3 / acetonitrile / 1 h / Ambient temperature 3: 90.6 percent / toluene / 15 h / Heating View Scheme
参考文献
Agathocleous, Demetrios C.; Bulman Page, Philip C.; Cosstick, Richard; Galpin, Ian J.; McLennan, Alexander G.; Prescott, Mark
Tetrahedron, 1990 , vol. 46, # 6 p. 2047 - 2058
反应条件
1: 80 percent / 0.25 h / 150 - 160 °C 2: 74.4 percent / CBr4/PPh3 / acetonitrile / 1 h / Ambient temperature 3: 90.6 percent / toluene / 15 h / Heating View Scheme
参考文献
Agathocleous, Demetrios C.; Bulman Page, Philip C.; Cosstick, Richard; Galpin, Ian J.; McLennan, Alexander G.; Prescott, Mark
Tetrahedron, 1990 , vol. 46, # 6 p. 2047 - 2058
反应条件
1: 74.4 percent / CBr4/PPh3 / acetonitrile / 1 h / Ambient temperature 2: 90.6 percent / toluene / 15 h / Heating View Scheme
参考文献
Agathocleous, Demetrios C.; Bulman Page, Philip C.; Cosstick, Richard; Galpin, Ian J.; McLennan, Alexander G.; Prescott, Mark
Tetrahedron, 1990 , vol. 46, # 6 p. 2047 - 2058
反应条件
1: caesium carbonate / acetonitrile / 80 °C 2: 0.5 h / Microwave irradiation View Scheme
参考文献
Long, Timothy E.; Lu, Xiao; Galizzi, Melina; Docampo, Roberto; Gut, Jiri; Rosenthal, Philip J.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2976 - 2979
反应条件
1: 1) t-BuOK / 1) -78 deg C, THF, 2a) -78 deg C, 7h, 2b) -78 deg C to RT, overnight
2: 39 percent / hydrazine hydrate / ethanol
3: 20 percent / pyridine / dimethylaminopyridine / Ambient temperature
4: 64 percent / methanolic ammonia
View Scheme
参考文献
Agathocleous, Demetrios C.; Bulman Page, Philip C.; Cosstick, Richard; Galpin, Ian J.; McLennan, Alexander G.; Prescott, Mark
Tetrahedron, 1990 , vol. 46, # 6 p. 2047 - 2058
