4-氯-2-二甲基氨基-1,3-噻唑-5-甲醛合成路线 (共 2 条)
反应条件
in tetrachloromethane T=20°C;
参考文献
Kotlyar; Pushkarev; Orlov; Chernenko; Desenko
Chemistry of Heterocyclic Compounds, 2010 , vol. 46, # 3 p. 334 - 341
反应条件
n-butyllithium 1) -78 deg C, 10 min., hexane, THF, 2) up to room temp., 2h; Yield given. Multistep reaction;
参考文献
Athmani, Salah; Bruce, Andrew; Iddon, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 2 p. 215 - 219