S-(三氟甲基)二苯并噻吩三氟甲基磺酸盐合成路线 （共 67 条）
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,6-di-tert-butyl-4-methylpyridine in 1,2-dichloro-ethane T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine in N,N-dimethyl acetamide T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302
反应条件
(2R,6S)-2,6-dimethylpiperidine in 1,2-dichloro-ethane T=20°C; 20 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 14 p. 4300 - 4302
反应条件
copper in acetonitrile T=60°C; 9 h; Inert atmosphere;
参考文献
Zhu, Lingui; Liu, Shasha; Douglas, Justin T.; Altman, Ryan A.
Chemistry - A European Journal, 2013 , vol. 19, # 38 p. 12800 - 12805
反应条件
copper in acetonitrile T=60°C; 9 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 38 p. 12800 - 12805
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
sodium hydride
1.) THF, 0 deg C, RT, 20 min, 2.) THF, RT, 0.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Umemoto, Teruo; Ishihara, Sumi
Journal of the American Chemical Society, 1993 , vol. 115, # 6 p. 2156 - 2164
反应条件
in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide
T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
