N-甲氧基-N-甲基-2-(三苯基磷)乙酰胺N-甲氧基-N-甲基-2-(三苯基磷)乙酰胺合成路线 (共 7 条)
反应条件
in acetonitrile 15 h; Heating;
参考文献
Evans; Kaldor; Jones; Clardy; Stout
Journal of the American Chemical Society, 1990 , vol. 112, # 19 p. 7001 - 7031
反应条件
1: in toluene T=80°C; Inert atmosphere; 2: With sodium hydroxide in dichloromethane; water T=20°C; Inert atmosphere;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Chippindale, Ann M.; Davies, Stephen G.; Iwamoto, Keiji; Parkin, Richard M.; Smethurst, Christian A. P.; Smith, Andrew D.; Rodriguez-Solla, Humberto
Tetrahedron, 2003 , vol. 59, # 18 p. 3253 - 3265
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 1,3-bis-(diphenylphosphino)propane; caesium carbonate in toluene
T=150°C; indirect Wittig reaction; 72 h;
参考文献
Edwards, Michael G.; Williams, Jonathan M.J.
Angewandte Chemie - International Edition, 2002 , vol. 41, # 24 p. 4740 - 4743
反应条件
in dimethyl sulfoxide
T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
manganese(IV) oxide in dichloromethane
21 h; Heating;
参考文献
Blackburn, Leonie; Kanno, Hisashi; Taylor, Richard J. K.
Tetrahedron Letters, 2003 , vol. 44, # 1 p. 115 - 118
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 1,3-bis-(diphenylphosphino)propane; caesium carbonate in toluene
T=150°C; indirect Wittig reaction; 72 h;
参考文献
Edwards, Michael G.; Williams, Jonathan M.J.
Angewandte Chemie - International Edition, 2002 , vol. 41, # 24 p. 4740 - 4743