反应条件
1.1: trichlorophosphate / N,N-dimethyl-formamide / 5 h / Reflux 1.2: 1 h / 0 - 5 °C 2.1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 120 °C 3.1: potassium hydroxide; [bis(acetoxy)iodo]benzene / methanol / Cooling with ice View Scheme
参考文献
Bouillot, Anne Marie Jeanne; Donche, Frederic; Gellibert, Francoise Jeanne; Lamotte, Yann; Mirguet, Olivier
Patent: US2012/232074 A1, 2012 ;
